John R. Dean
John Wiley & Sons
e druk, 2009
9780470772850
Extraction Techniques in Analytical Sciences
Specificaties
Gebonden, 308 blz.
|
Engels
John Wiley & Sons |
e druk, 2009
ISBN13: 9780470772850
Rubricering
Onderdeel van serie
Analytical Techniques in the Sciences (AnTs) ∗
Levertijd ongeveer 8 werkdagen
Samenvatting
Increasing environmental regulations have resulted in the need for new methods of analysis for environmental samples. As an updated version to
Extraction Methods for Environmental Analysis published in 1998,
Extraction Techniques in Analytical Science provides the fundamentals of extraction methods in environmental organic contaminants. The text explores topics like aqueous samples, solid samples, gaseous samples, comparisons of extraction methods, and resources. Also, the book discusses methods of analysis, including chromatographic approaches for environmental organic analysis. Written in the AnTS style, this text is ideal for students as a self–study guide.
Specificaties
Inhoudsopgave
Series Preface.
<p>Preface.</p>
<p>Acknowledgements.</p>
<p>Acronyms, Abbreviations and Symbols.</p>
<p>About the Author.</p>
<p>1 Pre– and Post–Extraction Considerations.</p>
<p>1.1 Introduction.</p>
<p>1.2 Organic Compounds of Interest.</p>
<p>1.3 Pre–Sampling Issues.</p>
<p>1.4 Sampling Strategies: Solid, Aqueous and Air Samples.</p>
<p>1.5 An Introduction to Practical Chromatographic Analysis.</p>
<p>1.6 Quality Assurance Aspects.</p>
<p>1.7 Health and Safety Considerations.</p>
<p>References.</p>
<p>AQUEOUS SAMPLES.</p>
<p>2 Classical Approaches for Aqueous Extraction.</p>
<p>2.1 Introduction.</p>
<p>2.2 Liquid Liquid Extraction.</p>
<p>2.3 Purge and Trap for Volatile Organics in Aqueous Samples.</p>
<p>References.</p>
<p>3 Solid Phase Extraction.</p>
<p>3.1 Introduction.</p>
<p>3.2 Types of SPE Media (Sorbent).</p>
<p>3.3 SPE Formats and Apparatus.</p>
<p>3.4 Method of SPE Operation.</p>
<p>3.5 Solvent Selection.</p>
<p>3.6 Factors Affecting SPE.</p>
<p>3.7 Selected Methods of Analysis for SPE.</p>
<p>3.8 Automation and On–Line SPE.</p>
<p>References.</p>
<p>4 Solid Phase Microextraction.</p>
<p>4.1 Introduction.</p>
<p>4.2 Theoretical Considerations.</p>
<p>4.3 Experimental.</p>
<p>4.4 Methods of Analysis: SPME GC.</p>
<p>4.5 Methods of Analysis: SPME HPLC MS.</p>
<p>4.6 Automation of SPME.</p>
<p>References.</p>
<p>5 New Developments in Microextraction.</p>
<p>5.1 Introduction.</p>
<p>5.2 Stir–Bar Sorptive Extraction (SBSE).</p>
<p>5.3 Liquid–Phase Microextraction.</p>
<p>5.4 Membrane Microextraction.</p>
<p>5.5 Microextraction in a Packed Syringe (MEPS).</p>
<p>References.</p>
<p>SOLID SAMPLES.</p>
<p>6 Classical Approaches for Solid Liquid Extraction.</p>
<p>6.1 Introduction.</p>
<p>6.2 Soxhlet Extraction.</p>
<p>6.3 Automated Soxhlet Extraction or Soxtec .</p>
<p>6.4 Other Approaches for Solid Liquid Extraction.</p>
<p>References.</p>
<p>7 Pressurized Fluid Extraction.</p>
<p>7.1 Introduction.</p>
<p>7.2 Theoretical Considerations Relating to the Extraction Process.</p>
<p>7.3 Instrumentation for PFE.</p>
<p>7.4 Method Development for PFE.</p>
<p>7.5 Applications of PFE.</p>
<p>7.6 Comparative Studies.</p>
<p>7.7 Miscellaneous.</p>
<p>References.</p>
<p>8 Microwave–Assisted Extraction.</p>
<p>8.1 Introduction.</p>
<p>8.2 Instrumentation.</p>
<p>8.3 Applications of MAE.</p>
<p>References.</p>
<p>9 Matrix Solid Phase Dispersion.</p>
<p>9.1 Introduction.</p>
<p>9.2 Issues on the Comparison of MSPD and SPE.</p>
<p>9.3 A Review of Selected Applications.</p>
<p>References.</p>
<p>10 Supercritical Fluid Extraction.</p>
<p>10.1 Introduction.</p>
<p>10.2 Instrumentation for SFE.</p>
<p>10.3 Applications of SFE.</p>
<p>10.4 Selection of SFE Operating Parameters.</p>
<p>References.</p>
<p>GASEOUS SAMPLES.</p>
<p>11 Air Sampling.</p>
<p>11.1 Introduction.</p>
<p>11.2 Techniques Used for Air Sampling.</p>
<p>References.</p>
<p>COMPARISON OF EXTRACTION METHODS.</p>
<p>12 Comparison of Extraction Methods.</p>
<p>12.1 Introduction.</p>
<p>12.2 Role of Certified Reference Materials.</p>
<p>12.3 Comparison of Extraction Techniques for (Semi)–Solid Samples.</p>
<p>12.4 Comparison of Extraction Techniques for Liquid Samples.</p>
<p>12.5 Comparison of Extraction Techniques for Air Sampling.</p>
<p>References.</p>
<p>RESOURCES.</p>
<p>13 Resources for Extraction Techniques.</p>
<p>13.1 Introduction.</p>
<p>13.2 Role of Worldwide Web.</p>
<p>Responses to Self–Assessment Questions.</p>
<p>Glossary of Terms.</p>
<p>SI Units and Physical Constants.</p>
<p>Periodic Table.</p>
<p>General Index.</p>
<p>Application Index.</p>
<p>Preface.</p>
<p>Acknowledgements.</p>
<p>Acronyms, Abbreviations and Symbols.</p>
<p>About the Author.</p>
<p>1 Pre– and Post–Extraction Considerations.</p>
<p>1.1 Introduction.</p>
<p>1.2 Organic Compounds of Interest.</p>
<p>1.3 Pre–Sampling Issues.</p>
<p>1.4 Sampling Strategies: Solid, Aqueous and Air Samples.</p>
<p>1.5 An Introduction to Practical Chromatographic Analysis.</p>
<p>1.6 Quality Assurance Aspects.</p>
<p>1.7 Health and Safety Considerations.</p>
<p>References.</p>
<p>AQUEOUS SAMPLES.</p>
<p>2 Classical Approaches for Aqueous Extraction.</p>
<p>2.1 Introduction.</p>
<p>2.2 Liquid Liquid Extraction.</p>
<p>2.3 Purge and Trap for Volatile Organics in Aqueous Samples.</p>
<p>References.</p>
<p>3 Solid Phase Extraction.</p>
<p>3.1 Introduction.</p>
<p>3.2 Types of SPE Media (Sorbent).</p>
<p>3.3 SPE Formats and Apparatus.</p>
<p>3.4 Method of SPE Operation.</p>
<p>3.5 Solvent Selection.</p>
<p>3.6 Factors Affecting SPE.</p>
<p>3.7 Selected Methods of Analysis for SPE.</p>
<p>3.8 Automation and On–Line SPE.</p>
<p>References.</p>
<p>4 Solid Phase Microextraction.</p>
<p>4.1 Introduction.</p>
<p>4.2 Theoretical Considerations.</p>
<p>4.3 Experimental.</p>
<p>4.4 Methods of Analysis: SPME GC.</p>
<p>4.5 Methods of Analysis: SPME HPLC MS.</p>
<p>4.6 Automation of SPME.</p>
<p>References.</p>
<p>5 New Developments in Microextraction.</p>
<p>5.1 Introduction.</p>
<p>5.2 Stir–Bar Sorptive Extraction (SBSE).</p>
<p>5.3 Liquid–Phase Microextraction.</p>
<p>5.4 Membrane Microextraction.</p>
<p>5.5 Microextraction in a Packed Syringe (MEPS).</p>
<p>References.</p>
<p>SOLID SAMPLES.</p>
<p>6 Classical Approaches for Solid Liquid Extraction.</p>
<p>6.1 Introduction.</p>
<p>6.2 Soxhlet Extraction.</p>
<p>6.3 Automated Soxhlet Extraction or Soxtec .</p>
<p>6.4 Other Approaches for Solid Liquid Extraction.</p>
<p>References.</p>
<p>7 Pressurized Fluid Extraction.</p>
<p>7.1 Introduction.</p>
<p>7.2 Theoretical Considerations Relating to the Extraction Process.</p>
<p>7.3 Instrumentation for PFE.</p>
<p>7.4 Method Development for PFE.</p>
<p>7.5 Applications of PFE.</p>
<p>7.6 Comparative Studies.</p>
<p>7.7 Miscellaneous.</p>
<p>References.</p>
<p>8 Microwave–Assisted Extraction.</p>
<p>8.1 Introduction.</p>
<p>8.2 Instrumentation.</p>
<p>8.3 Applications of MAE.</p>
<p>References.</p>
<p>9 Matrix Solid Phase Dispersion.</p>
<p>9.1 Introduction.</p>
<p>9.2 Issues on the Comparison of MSPD and SPE.</p>
<p>9.3 A Review of Selected Applications.</p>
<p>References.</p>
<p>10 Supercritical Fluid Extraction.</p>
<p>10.1 Introduction.</p>
<p>10.2 Instrumentation for SFE.</p>
<p>10.3 Applications of SFE.</p>
<p>10.4 Selection of SFE Operating Parameters.</p>
<p>References.</p>
<p>GASEOUS SAMPLES.</p>
<p>11 Air Sampling.</p>
<p>11.1 Introduction.</p>
<p>11.2 Techniques Used for Air Sampling.</p>
<p>References.</p>
<p>COMPARISON OF EXTRACTION METHODS.</p>
<p>12 Comparison of Extraction Methods.</p>
<p>12.1 Introduction.</p>
<p>12.2 Role of Certified Reference Materials.</p>
<p>12.3 Comparison of Extraction Techniques for (Semi)–Solid Samples.</p>
<p>12.4 Comparison of Extraction Techniques for Liquid Samples.</p>
<p>12.5 Comparison of Extraction Techniques for Air Sampling.</p>
<p>References.</p>
<p>RESOURCES.</p>
<p>13 Resources for Extraction Techniques.</p>
<p>13.1 Introduction.</p>
<p>13.2 Role of Worldwide Web.</p>
<p>Responses to Self–Assessment Questions.</p>
<p>Glossary of Terms.</p>
<p>SI Units and Physical Constants.</p>
<p>Periodic Table.</p>
<p>General Index.</p>
<p>Application Index.</p>